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Vol. 6, Issue 2 (2017)

UHPLC detection of OTC residues in swine tissues

R Gogoi and DC Roy
A study was undertaken to detect residues of Oxytetracycline (OTC) in swine tissues using Ultra High Performance Liquid Chromatography (UHPLC) system. A total of 216 nos. of representative swine tissue samples were collected from pork markets and roadside meat stalls of Assam. The samples after collection were preserved at -20 °C and then screened by UHPLC with Diode Array Detector (DAD). OTC residues were extracted with EDTA-McIIvaine buffer. Solid phase extraction clean-up was done with SPE C18 cartridge. Recovery ranged from 94-98%. A total of 5 nos. of the screened samples were detected to be positive for trace residues of OTC, 2 above the Maximum Residue Limit (MRL). It may be concluded that the present method reliably and precisely detects OTC residue in swine tissues.
Pages: 97-99  |  2910 Views  129 Downloads

The Pharma Innovation Journal
How to cite this article:
R Gogoi, DC Roy. UHPLC detection of OTC residues in swine tissues. Pharma Innovation 2017;6(2):97-99.

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